Data DOI: 10.15785/SBGRID/89 | ID: 89
Publication DOI: 10.1172/JCI64896
4EYM Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB
Brett Laboratory, Washington U. School of Medicine
Release Date: May 19, 2015
1. If this dataset is locally available, it should be accessable at /programs/datagrid/89
2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:
'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/89 .' (Harvard Medical School, USA)
Depending on your location, faster access may be available from a Tier 1 site closer to your location
'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/89 .' (Uppsala University, Sweden)
'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/89 .' (Institut Pasteur de Montevideo, Uruguay)
'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/89 .' (Shanghai Institutes for Biological Sciences, China)
3. After the transfer is completed, please issue the following command to verify data integrity:
'cd 89 ; shasum -c files.sha'
Storage requirements: 1.5G
Biological Sample:
MAPK13 in complex with inhibitor 124
Dataset Type:
X-Ray Diffraction
Subject Composition:
Ligand, Protein
Collection Facility:
ALS 4.2.2
Data Creation Date:
Sept. 29, 2011
Related Datasets:
None
Brett, TJ; Brett, T. 2015. "X-Ray Diffraction data for: MAPK13 in complex with inhibitor 124. PDB Code 4EYM", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/89.
hi res data
| Name | Additional Roles | Affiliation While Working on the Project |
|---|---|---|
| Thomas J Brett | Data Collector, Depositor | Washington University School of Medicine |
| Tom Brett | PI | Washington U. School of Medicine |
HKL2000
Version:
version unreported
Reprocessing failed.
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 1.038
Sweep:
SWEEP1
Files:
/programs/datagrid/89/d124_5_1_###.img
Images:
1 - 180
Beam:
(79.07, 77.9) -> (79.07, 77.75)
Distance:
-150.0 -> -150.08
Spacegroup:
P 21 21 21
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 2.23 | 6.05 | 2.23 |
| Low resolution limit | 38.77 | 38.78 | 2.27 |
| Completeness | 96.3 | 100.0 | 98.8 |
| Multiplicity | 6.3 | 6.0 | 6.0 |
| I/sigma | 13.3 | 23.3 | 25.9 |
| Rmerge | 0.103 | 0.046 | 0.1 |
| CC half | 0.991 | 0.999 | 0.977 |
| Anomalous completeness | 92.6 | 99.7 | 94.6 |
| Anomalous multiplicity | 3.4 | 3.4 | 3.4 |
| Cell | 61.22 | 69.68 | 93.32 | 90.0 | 90.0 | 90.0 |
|---|
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 1.038
Sweep:
SWEEP1
Files:
/programs/datagrid/89/d124_5_1_###.img
Images:
1 - 180
Beam:
(79.07, 77.9) -> (79.07, 77.75)
Distance:
-150.0 -> -150.02
Spacegroup:
P 21 21 21
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 2.22 | 6.02 | 2.22 |
| Low resolution limit | 51.2 | 51.21 | 2.26 |
| Completeness | 96.1 | 100.0 | 96.8 |
| Multiplicity | 6.2 | 6.0 | 5.4 |
| I/sigma | 13.6 | 23.4 | 21.1 |
| Rmerge | 0.101 | 0.045 | 0.098 |
| CC half | 0.991 | 0.995 | 0.984 |
| Anomalous completeness | 92.0 | 99.9 | 86.6 |
| Anomalous multiplicity | 3.4 | 3.4 | 3.4 |
| Cell | 61.23 | 69.69 | 93.33 | 90.0 | 90.0 | 90.0 |
|---|
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 1.038
Sweep:
SWEEP1
Files:
/programs/datagrid/89/d124_5_1_###.img
Images:
1 - 180
Beam:
(79.07, 77.9) -> (79.07, 77.72)
Distance:
-150.0 -> -150.3
Spacegroup:
P 1
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 2.27 | 6.16 | 2.27 |
| Low resolution limit | 55.91 | 55.92 | 2.31 |
| Completeness | 92.6 | 99.4 | 76.1 |
| Multiplicity | 1.9 | 1.9 | 1.7 |
| I/sigma | 5.7 | 18.5 | 2.2 |
| Rmerge | 0.303 | 0.108 | 0.667 |
| CC half | 0.875 | 0.947 | 0.447 |
| Anomalous completeness | 71.3 | 88.5 | 43.2 |
| Anomalous multiplicity | 1.1 | 1.1 | 1.1 |
| Cell | 61.411 | 69.984 | 93.744 | 90.003 | 90.04 | 89.969 |
|---|
License: CC0
Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.
