Data DOI: 10.15785/SBGRID/89 | ID: 89
Publication DOI: 10.1172/JCI64896
4EYM Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB
Brett Laboratory, Washington U. School of Medicine
Release Date: May 19, 2015
1. If this dataset is locally available, it should be accessable at /programs/datagrid/89
2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:
'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/89 .' (Harvard Medical School, USA)
Depending on your location, faster access may be available from a Tier 1 site closer to your location
'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/89 .' (Uppsala University, Sweden)
'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/89 .' (Institut Pasteur de Montevideo, Uruguay)
'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/89 .' (Shanghai Institutes for Biological Sciences, China)
3. After the transfer is completed, please issue the following command to verify data integrity:
'cd 89 ; shasum -c files.sha'
Storage requirements: 1.5G
Biological Sample:
MAPK13 in complex with inhibitor 124
Dataset Type:
X-Ray Diffraction
Subject Composition:
Ligand, Protein
Collection Facility:
ALS 4.2.2
Data Creation Date:
Sept. 29, 2011
Related Datasets:
None
Brett, TJ; Brett, T. 2015. "X-Ray Diffraction data for: MAPK13 in complex with inhibitor 124. PDB Code 4EYM", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/89.
hi res data
| Name | Additional Roles | Affiliation While Working on the Project |
|---|---|---|
| Thomas J Brett | Data Collector, Depositor | Washington University School of Medicine |
| Tom Brett | PI | Washington U. School of Medicine |
HKL2000
Version:
version unreported
Reprocessing failed.
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 1.038
Sweep:
SWEEP1
Files:
/programs/datagrid/89/d124_5_1_###.img
Images:
1 - 180
Beam:
(79.07, 77.9) -> (79.07, 77.75)
Distance:
-150.0 -> -150.15
Spacegroup:
P 21 21 21
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 2.13 | 5.78 | 2.13 |
| Low resolution limit | 38.74 | 38.75 | 2.17 |
| Completeness | 93.3 | 100.0 | 57.7 |
| Multiplicity | 6.0 | 6.1 | 2.3 |
| I/sigma | 12.4 | 23.5 | 1.3 |
| Rmerge | 0.097 | 0.043 | 0.467 |
| CC half | 0.992 | 0.998 | 0.667 |
| Anomalous completeness | 86.9 | 99.4 | 34.4 |
| Anomalous multiplicity | 3.3 | 3.3 | 3.3 |
| Cell | 61.18 | 69.63 | 93.26 | 90.0 | 90.0 | 90.0 |
|---|
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 1.038
Sweep:
SWEEP1
Files:
/programs/datagrid/89/d124_5_1_###.img
Images:
1 - 180
Beam:
(79.07, 77.9) -> (79.07, 77.75)
Distance:
-150.0 -> -150.02
Spacegroup:
P 21 21 21
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 2.13 | 5.78 | 2.13 |
| Low resolution limit | 51.16 | 51.18 | 2.17 |
| Completeness | 93.8 | 100.0 | 58.9 |
| Multiplicity | 6.0 | 6.1 | 2.3 |
| I/sigma | 12.1 | 23.4 | 1.3 |
| Rmerge | 0.099 | 0.046 | 0.459 |
| CC half | 0.991 | 0.997 | 0.436 |
| Anomalous completeness | 87.5 | 99.7 | 35.3 |
| Anomalous multiplicity | 3.3 | 3.3 | 3.3 |
| Cell | 61.19 | 69.65 | 93.28 | 90.0 | 90.0 | 90.0 |
|---|
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 1.038
Sweep:
SWEEP1
Files:
/programs/datagrid/89/d124_5_1_###.img
Images:
1 - 180
Beam:
(79.07, 77.9) -> (79.07, 77.72)
Distance:
-150.0 -> -150.15
Spacegroup:
P 1 2 1
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 2.23 | 6.05 | 2.23 |
| Low resolution limit | 69.62 | 69.66 | 2.27 |
| Completeness | 98.9 | 99.9 | 93.9 |
| Multiplicity | 3.6 | 3.6 | 3.5 |
| I/sigma | 4.0 | 5.1 | 6.5 |
| Rmerge | 0.205 | 0.151 | 0.197 |
| CC half | 0.935 | 0.884 | 0.792 |
| Anomalous completeness | 96.7 | 98.5 | 90.0 |
| Anomalous multiplicity | 1.9 | 1.9 | 1.9 |
| Cell | 61.109 | 69.622 | 93.244 | 90.0 | 90.029 | 90.0 |
|---|
License: CC0
Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.
