X-Ray Diffraction data from MAPK13 in complex with inhibitor 124, source of 4EYM structure

Data DOI: 10.15785/SBGRID/89 | ID: 89

Publication DOI: 10.1172/JCI64896

4EYM Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Brett Laboratory, Washington U. School of Medicine

Release Date: May 19, 2015

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/89

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/89 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/89 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/89 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/89 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 89 ; shasum -c files.sha'

Storage requirements: 1.5G

Biological Sample:

MAPK13 in complex with inhibitor 124

Dataset Type:

X-Ray Diffraction

Subject Composition:

Ligand, Protein

Collection Facility:

ALS 4.2.2

Data Creation Date:

Sept. 29, 2011

Related Datasets:

None


Cite this Dataset

Brett, TJ; Brett, T. 2015. "X-Ray Diffraction data for: MAPK13 in complex with inhibitor 124. PDB Code 4EYM", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/89.

Download Citation

Dataset Description

hi res data

Project Members

Name Additional Roles Affiliation While Working on the Project
Thomas J BrettData Collector, DepositorWashington University School of Medicine
Tom BrettPIWashington U. School of Medicine

Reprocessing Instructions

HKL2000

Reprocessing Data

About Reprocessing

Version:

version unreported

Reprocessing failed.

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.038

Sweep:

SWEEP1

Files:

/programs/datagrid/89/d124_5_1_###.img

Images:

1 - 180

Beam:

(79.07, 77.9) -> (79.07, 77.75)

Distance:

-150.0 -> -150.15

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.13 5.78 2.13
Low resolution limit 38.74 38.75 2.17
Completeness 93.3 100.0 57.7
Multiplicity 6.0 6.1 2.3
I/sigma 12.4 23.5 1.3
Rmerge 0.097 0.043 0.467
CC half 0.992 0.998 0.667
Anomalous completeness 86.9 99.4 34.4
Anomalous multiplicity 3.3 3.3 3.3
Cell 61.18 69.63 93.26 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.038

Sweep:

SWEEP1

Files:

/programs/datagrid/89/d124_5_1_###.img

Images:

1 - 180

Beam:

(79.07, 77.9) -> (79.07, 77.75)

Distance:

-150.0 -> -150.02

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.13 5.78 2.13
Low resolution limit 51.16 51.18 2.17
Completeness 93.8 100.0 58.9
Multiplicity 6.0 6.1 2.3
I/sigma 12.1 23.4 1.3
Rmerge 0.099 0.046 0.459
CC half 0.991 0.997 0.436
Anomalous completeness 87.5 99.7 35.3
Anomalous multiplicity 3.3 3.3 3.3
Cell 61.19 69.65 93.28 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.038

Sweep:

SWEEP1

Files:

/programs/datagrid/89/d124_5_1_###.img

Images:

1 - 180

Beam:

(79.07, 77.9) -> (79.07, 77.72)

Distance:

-150.0 -> -150.15

Spacegroup:

P 1 2 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.23 6.05 2.23
Low resolution limit 69.62 69.66 2.27
Completeness 98.9 99.9 93.9
Multiplicity 3.6 3.6 3.5
I/sigma 4.0 5.1 6.5
Rmerge 0.205 0.151 0.197
CC half 0.935 0.884 0.792
Anomalous completeness 96.7 98.5 90.0
Anomalous multiplicity 1.9 1.9 1.9
Cell 61.109 69.622 93.244 90.0 90.029 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.