Data DOI: 10.15785/SBGRID/86 | ID: 86
Publication DOI: 10.1016/j.cell.2014.03.061
4PK2 Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB
Roll-Mecak Laboratory, National Institutes of Health
Release Date: 19 May 2015
1. If this dataset is locally available, it should be accessable at /programs/datagrid/86
2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:
'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/86 .' (Harvard Medical School, USA)
Depending on your location, faster access may be available from a Tier 1 site closer to your location
'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/86 .' (Uppsala University, Sweden)
'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/86 .' (Institut Pasteur de Montevideo, Uruguay)
'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/86 .' (Shanghai Institutes for Biological Sciences, China)
3. After the transfer is completed, please issue the following command to verify data integrity:
'cd 86 ; shasum -c files.sha'
Storage requirements: 4.4G
Biological Sample:
Human Tubulin Acetyltransferase in complex with bisubstrate analog
Dataset Type:
X-Ray Diffraction
Subject Composition:
Ligand, Protein
Collection Facility:
Advanced Light Source (ALS), beamline 5.0.1.
Data Creation Date:
12 Nov 2012
Related Datasets:
None
Szyk, A; Roll-Mecak, A. 2015. "X-Ray Diffraction data for: Human Tubulin Acetyltransferase in complex with bisubstrate analog. PDB Code 4PK2", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/86.
Native data set
| Name | Additional Roles | Affiliation While Working on the Project |
|---|---|---|
| Agnieszka Szyk | Data Collector, Depositor | NIH/NINDS |
| Antonina Roll-Mecak | PI | National Institutes of Health |
The data set was indexed in P21 space group, 250 frames were processed with HKL2000 at 1.35A resolution
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 1.0
Sweep:
SWEEP1
Files:
/programs/datagrid/86/arm5_9_8_###.img
Images:
1 - 250
Beam:
(154.49, 161.6) -> (154.49, 161.59)
Distance:
180.0 -> 179.98
Spacegroup:
P 1 21 1
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 1.16 | 3.13 | 1.16 |
| Low resolution limit | 23.92 | 23.93 | 1.18 |
| Completeness | 72.8 | 99.2 | 5.0 |
| Multiplicity | 4.6 | 4.9 | 1.1 |
| I/sigma | 16.7 | 37.6 | 0.4 |
| Rmerge | 0.036 | 0.024 | 1.875 |
| CC half | 0.999 | 0.999 | 0.023 |
| Anomalous completeness | 68.6 | 97.2 | 0.2 |
| Anomalous multiplicity | 2.4 | 2.4 | 2.4 |
| Cell | 37.02 | 52.01 | 50.0 | 90.0 | 106.9 | 90.0 |
|---|
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 1.0
Sweep:
SWEEP1
Files:
/programs/datagrid/86/arm5_9_8_###.img
Images:
1 - 250
Beam:
(154.49, 161.6) -> (154.49, 161.58)
Distance:
180.0 -> 180.04
Spacegroup:
P 1 21 1
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 1.16 | 3.14 | 1.16 |
| Low resolution limit | 35.21 | 35.23 | 1.18 |
| Completeness | 72.8 | 99.1 | 5.0 |
| Multiplicity | 4.6 | 4.9 | 1.1 |
| I/sigma | 16.7 | 37.6 | 0.4 |
| Rmerge | 0.036 | 0.024 | 1.885 |
| CC half | 0.999 | 0.999 | 0.009 |
| Anomalous completeness | 68.6 | 97.2 | 0.2 |
| Anomalous multiplicity | 2.4 | 2.4 | 2.4 |
| Cell | 37.02 | 52.01 | 50.0 | 90.0 | 106.9 | 90.0 |
|---|
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 1.0
Sweep:
SWEEP1
Files:
/programs/datagrid/86/arm5_9_8_###.img
Images:
1 - 250
Beam:
(154.49, 161.6) -> (154.49, 161.59)
Distance:
180.0 -> 179.91
Spacegroup:
P 1 21 1
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 1.34 | 3.64 | 1.34 |
| Low resolution limit | 52.01 | 52.05 | 1.36 |
| Completeness | 95.3 | 100.0 | 66.2 |
| Multiplicity | 4.9 | 5.2 | 3.7 |
| I/sigma | 14.9 | 52.6 | 24.0 |
| Rmerge | 0.085 | 0.032 | 0.133 |
| CC half | 0.984 | 0.998 | 0.214 |
| Anomalous completeness | 94.0 | 100.0 | 60.4 |
| Anomalous multiplicity | 2.5 | 2.5 | 2.5 |
| Cell | 36.99 | 52.014 | 49.994 | 90.0 | 106.857 | 90.0 |
|---|
License: CC0
Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.
