X-Ray Diffraction data from RPA70N in complex with a 3,4 dichlorophenylalanine ATRIP derived peptide, source of 4NB3 structure

Data DOI: 10.15785/SBGRID/66 | ID: 66

Publication DOI: 10.1021/jm401730y

4NB3 Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Chazin Laboratory, Vanderbilt University

Release Date: May 7, 2015

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/66

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/66 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/66 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/66 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/66 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 66 ; shasum -c files.sha'

Storage requirements: 15G

Biological Sample:

RPA70N in complex with a 3,4 dichlorophenylalanine ATRIP derived peptide

Dataset Type:

X-Ray Diffraction

Subject Composition:

Protein

Collection Facility:

21-ID-G, LS-CAT, APS, Chicago, IL

Data Creation Date:

Oct. 22, 2012

Related Datasets:

None


Cite this Dataset

Feldkamp, MD; Chazin, W. 2015. "X-Ray Diffraction data for: RPA70N in complex with a 3,4 dichlorophenylalanine ATRIP derived peptide. PDB Code 4NB3", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/66.

Download Citation

Dataset Description

Native dataset

Project Members

Name Additional Roles Affiliation While Working on the Project
Michael D FeldkampData Collector, DepositorVanderbilt University
Walter J. ChazinPIVanderbilt University

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/66/CL036_1.###

Images:

1 - 450

Beam:

(145.2, 155.65) -> (145.2, 155.52)

Distance:

150.0 -> 149.95

Spacegroup:

C 1 2 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.24 3.37 1.24
Low resolution limit 40.04 40.06 1.26
Completeness 99.9 98.9 99.9
Multiplicity 7.2 7.3 5.3
I/sigma 8.4 20.2 1.2
Rmerge 0.089 0.05 1.203
CC half 0.997 0.996 0.563
Anomalous completeness 99.8 98.2 98.7
Anomalous multiplicity 3.7 3.7 3.7
Cell 89.978 46.782 78.708 90.0 120.608 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/66/CL036_1.###

Images:

1 - 450

Beam:

(145.2, 155.65) -> (145.2, 155.53)

Distance:

150.0 -> 149.84

Spacegroup:

C 1 2 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.24 3.36 1.24
Low resolution limit 30.09 30.1 1.26
Completeness 99.8 99.8 99.5
Multiplicity 7.1 7.1 5.4
I/sigma 12.7 32.3 1.1
Rmerge 0.061 0.043 1.32
CC half 0.997 0.996 0.526
Anomalous completeness 99.6 99.4 98.5
Anomalous multiplicity 3.6 3.6 3.6
Cell 90.13 46.82 78.82 90.0 120.65 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/66/CL036_1.###

Images:

1 - 450

Beam:

(145.2, 155.65) -> (145.2, 155.53)

Distance:

150.0 -> 149.97

Spacegroup:

C 1 2 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.24 3.37 1.24
Low resolution limit 40.08 40.1 1.26
Completeness 99.8 99.8 99.6
Multiplicity 7.1 7.1 5.4
I/sigma 12.7 32.3 1.1
Rmerge 0.061 0.043 1.321
CC half 0.997 0.996 0.53
Anomalous completeness 99.6 99.4 98.5
Anomalous multiplicity 3.6 3.6 3.6
Cell 90.13 46.82 78.82 90.0 120.65 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/66/CL036_1.###

Images:

1 - 450

Beam:

(145.2, 155.65) -> (145.2, 155.62)

Distance:

150.0 -> 149.85

Spacegroup:

C 1 2 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.28 3.47 1.28
Low resolution limit 40.05 40.07 1.3
Completeness 99.7 98.7 96.3
Multiplicity 7.3 7.3 5.8
I/sigma 9.1 26.4 1.1
Rmerge 0.078 0.046 1.032
CC half 0.998 0.998 0.74
Anomalous completeness 99.7 98.1 96.1
Anomalous multiplicity 3.7 3.7 3.7
Cell 90.052 46.784 78.716 90.0 120.671 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.