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The SBDB will be operating at a reduced level due to underlying network maintenance, starting July 24. New dataset registrations, deposition credential requests, dataset uploads, and dataset downloads from HMS will be unavailable during this time. Local access and downloads from other DAA sites will be unaffected. We expect to return to full operations July 25 or earlier.

X-Ray Diffraction data from PEAK1 (Sugen Kinase 269, SgK269), source of 6BHC structure

Data DOI: 10.15785/SBGRID/514 | ID: 514

Publication DOI: 10.1074/jbc.RA117.000751

6BHC Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Boggon Laboratory, Yale University School of Medicine

Release Date: Dec. 12, 2017

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/514

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/514 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/514 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/514 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/514 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 514 ; shasum -c files.sha'

Storage requirements: 6.1G

Biological Sample:

PEAK1 (Sugen Kinase 269, SgK269)

Dataset Type:

X-Ray Diffraction

Subject Composition:

Protein

Collection Facility:

APS 24-ID-E

Data Creation Date:

July 31, 2017

Related Datasets:

None


Cite this Dataset

Ha, BHak; Boggon, TJ. 2017. "X-Ray Diffraction data for: PEAK1 (Sugen Kinase 269, SgK269). PDB Code 6BHC", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/514.

Download Citation

Dataset Description

360 images

Project Members

Name Additional Roles Affiliation While Working on the Project
Titus J BoggonDepositorYale University
Byung Hak HaData CollectorYale University
Titus BoggonPIYale University School of Medicine

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97918

Sweep:

SWEEP1

Files:

/programs/datagrid/514/TJB3P03_1_######.cbf

Images:

1 - 360

Beam:

(163.7, 154.86) -> (163.7, 154.81)

Distance:

270.0 -> 269.57

Spacegroup:

P 21 21 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.53 6.87 2.53
Low resolution limit 72.59 72.62 2.57
Completeness 99.4 100.0 99.1
Multiplicity 6.1 6.0 6.0
I/sigma 6.5 11.1 2.4
Rmerge 0.271 0.081 2.161
CC half 0.98 0.993 0.257
Anomalous completeness 97.7 100.0 95.6
Anomalous multiplicity 3.3 3.3 3.3
Cell 72.59 103.037 58.68 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97918

Sweep:

SWEEP1

Files:

/programs/datagrid/514/TJB3P03_1_######.cbf

Images:

1 - 360

Beam:

(163.7, 154.86) -> (163.7, 154.73)

Distance:

270.0 -> 269.02

Spacegroup:

P 21 21 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 3.12 8.43 3.12
Low resolution limit 34.17 34.17 3.17
Completeness 99.8 99.8 99.7
Multiplicity 6.3 5.9 6.1
I/sigma 17.8 26.1 9.0
Rmerge 0.077 0.047 0.239
CC half 0.997 0.998 0.973
Anomalous completeness 98.2 98.3 98.0
Anomalous multiplicity 3.5 3.5 3.5
Cell 72.45 102.79 58.65 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97918

Sweep:

SWEEP1

Files:

/programs/datagrid/514/TJB3P03_1_######.cbf

Images:

1 - 360

Beam:

(163.7, 154.86) -> (163.7, 154.76)

Distance:

270.0 -> 277.03

Spacegroup:

P 21 21 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.27 6.16 2.27
Low resolution limit 72.44 72.48 2.31
Completeness 99.7 99.1 99.3
Multiplicity 6.5 5.9 6.3
I/sigma 8.6 21.6 1.3
Rmerge 0.133 0.054 1.713
CC half 0.996 0.997 0.262
Anomalous completeness 98.4 96.3 98.1
Anomalous multiplicity 3.5 3.5 3.5
Cell 72.44 102.78 58.65 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97918

Sweep:

SWEEP1

Files:

/programs/datagrid/514/TJB3P03_1_######.cbf

Images:

1 - 360

Beam:

(163.7, 154.86) -> (163.7, 154.74)

Distance:

270.0 -> 267.87

Spacegroup:

P 1 21 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.52 6.83 2.52
Low resolution limit 72.54 72.57 2.56
Completeness 99.3 100.0 96.2
Multiplicity 3.5 3.6 3.5
I/sigma 5.8 9.9 2.3
Rmerge 0.15 0.053 1.149
CC half 0.98 0.993 0.287
Anomalous completeness 95.1 99.9 92.3
Anomalous multiplicity 1.8 1.8 1.8
Cell 58.678 102.873 72.536 90.053 90.0 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.