X-Ray Diffraction data from PAK4, source of 5VEE structure

Data DOI: 10.15785/SBGRID/493 | ID: 493

Publication DOI: 10.1016/j.bbapap.2017.10.004

5VEE Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Boggon Laboratory, Yale University School of Medicine

Release Date: Oct. 13, 2017

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/493

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/493 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/493 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/493 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/493 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 493 ; shasum -c files.sha'

Storage requirements: 6.4G

Biological Sample:

PAK4

Dataset Type:

X-Ray Diffraction

Subject Composition:

Protein

Collection Facility:

APS 24-ID-E

Data Creation Date:

March 10, 2016

Related Datasets:

None


Cite this Dataset

Ha, BHak; Zhang, EY; Boggon, TJ. 2017. "X-Ray Diffraction data for: PAK4. PDB Code 5VEE", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/493.

Download Citation

Dataset Description

2 180 degree sweeps

Project Members

Name Additional Roles Affiliation While Working on the Project
Titus J BoggonData Collector, DepositorYale University
Byung Hak HaData CollectorYale University
Eric Y ZhangData CollectorYale University
Titus BoggonPIYale University School of Medicine

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97919

Sweep:

SWEEP2

Files:

/programs/datagrid/493/TJB14_9_EZqp_1_###.img

Images:

1 - 180

Beam:

(150.56, 158.89) -> (150.56, 158.94)

Distance:

280.0 -> 280.47

Spacegroup:

P 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.34 6.35 2.34
Low resolution limit 63.15 63.18 2.38
Completeness 93.7 95.1 93.7
Multiplicity 2.0 2.9 1.9
I/sigma 3.6 10.2 0.4
Rmerge 0.078 0.065 1.618
CC half 0.995 0.998 0.325
Anomalous completeness 69.1 87.6 68.4
Anomalous multiplicity 1.1 1.1 1.1
Cell 63.103 63.154 184.056 89.982 89.989 89.935

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97919

Sweep:

SWEEP2

Files:

/programs/datagrid/493/TJB14_9_EZqp_1_###.img

Images:

1 - 180

Beam:

(150.56, 158.89) -> (150.56, 158.88)

Distance:

280.0 -> 279.17

Spacegroup:

P 41 21 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.54 6.89 2.54
Low resolution limit 43.39 43.39 2.58
Completeness 100.0 100.0 99.8
Multiplicity 16.6 15.4 14.3
I/sigma 27.6 74.0 1.7
Rmerge 0.057 0.027 1.567
CC half 1.0 1.0 0.885
Anomalous completeness 99.6 99.5 99.4
Anomalous multiplicity 9.2 9.2 9.2
Cell 63.14 63.14 184.02 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97919

Sweep:

SWEEP2

Files:

/programs/datagrid/493/TJB14_9_EZqp_1_###.img

Images:

1 - 180

Beam:

(150.56, 158.89) -> (150.56, 158.88)

Distance:

280.0 -> 279.87

Spacegroup:

P 41 21 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.37 6.43 2.37
Low resolution limit 52.06 52.07 2.41
Completeness 99.3 100.0 85.9
Multiplicity 15.9 16.9 13.9
I/sigma 23.2 74.0 0.6
Rmerge 0.058 0.029 3.83
CC half 1.0 1.0 0.67
Anomalous completeness 98.8 99.6 83.2
Anomalous multiplicity 8.8 8.8 8.8
Cell 63.14 63.14 184.03 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97919

Sweep:

SWEEP2

Files:

/programs/datagrid/493/TJB14_9_EZqp_1_###.img

Images:

1 - 180

Beam:

(150.56, 158.89) -> (150.56, 158.87)

Distance:

280.0 -> 279.24

Spacegroup:

P 41 21 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.37 6.44 2.37
Low resolution limit 61.12 61.14 2.42
Completeness 100.0 100.0 100.0
Multiplicity 20.8 17.5 13.9
I/sigma 14.6 31.1 0.9
Rmerge 0.115 0.041 2.267
CC half 0.999 0.999 0.818
Anomalous completeness 100.0 99.6 100.0
Anomalous multiplicity 11.5 11.5 11.5
Cell 62.943 62.943 183.347 90.0 90.0 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.