X-Ray Diffraction data from Mycobacterial glucosylglycerate hydrolase - E419A mutant in complex with glucosylglycolate, source of 5OO2 structure

Data DOI: 10.15785/SBGRID/483 | ID: 483

Publication DOI: 10.1107/S2052252519005372

5OO2 Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Pereira Laboratory, IBMC/i3S, Universidade do Porto

Release Date: May 3, 2019

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/483

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/483 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/483 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/483 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/483 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 483 ; shasum -c files.sha'

Storage requirements: 5.7G

Biological Sample:

Mycobacterial glucosylglycerate hydrolase - E419A mutant in complex with glucosylglycolate

Dataset Type:

X-Ray Diffraction

Subject Composition:

Ligand, Protein

Collection Facility:

SOLEIL PROXIMA2

Data Creation Date:

July 9, 2016

Related Datasets:

None


Cite this Dataset

Cereija, TB.; Pereira, PJ.B.. 2019. "X-Ray Diffraction data for: Mycobacterial glucosylglycerate hydrolase - E419A mutant in complex with glucosylglycolate. PDB Code 5OO2", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/483.

Download Citation

Dataset Description

X-Ray Diffraction data from M. hassiacum GgH, source of 5OO2 structure

Project Members

Name Additional Roles Affiliation While Working on the Project
Pedro J.B. PereiraDepositorIBMC - Instituto de Biologia Molecular e Celular
Tatiana B. CereijaData CollectorIBMC - Instituto de Biologia Molecular e Celular
Pedro PereiraPIUniversidade do Porto

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Reprocessing failed.

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.98011

Sweep:

SWEEP1

Files:

/programs/datagrid/483/BH3783_1_master.h5

Images:

1 - 1800

Beam:

(123.95, 115.49) -> (123.95, 115.46)

Distance:

189.59 -> 190.4

Spacegroup:

P 21 21 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.1 5.7 2.1
Low resolution limit 40.03 40.03 2.14
Completeness 100.0 100.0 100.0
Multiplicity 6.6 6.7 6.9
I/sigma 8.5 21.6 1.3
Rmerge 0.108 0.056 1.331
CC half 0.996 0.996 0.597
Anomalous completeness 98.5 99.5 99.4
Anomalous multiplicity 3.5 3.5 3.5
Cell 157.74 87.0 87.59 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.98011

Sweep:

SWEEP1

Files:

/programs/datagrid/483/BH3783_1_master.h5

Images:

1 - 1800

Beam:

(123.95, 115.49) -> (123.95, 115.46)

Distance:

189.59 -> 190.12

Spacegroup:

P 21 21 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.12 5.75 2.12
Low resolution limit 42.2 42.21 2.16
Completeness 99.9 100.0 99.9
Multiplicity 6.6 6.7 6.9
I/sigma 8.8 21.9 1.3
Rmerge 0.106 0.055 1.293
CC half 0.996 0.997 0.593
Anomalous completeness 98.3 99.5 99.2
Anomalous multiplicity 3.5 3.5 3.5
Cell 157.76 87.02 87.6 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.98011

Sweep:

SWEEP1

Files:

/programs/datagrid/483/BH3783_1_master.h5

Images:

1 - 1800

Beam:

(123.95, 115.49) -> (123.95, 115.47)

Distance:

189.59 -> 189.83

Spacegroup:

P 21 21 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.07 5.62 2.07
Low resolution limit 87.8 87.88 2.1
Completeness 100.0 100.0 99.1
Multiplicity 6.6 6.9 6.7
I/sigma 4.8 9.9 1.2
Rmerge 0.195 0.083 1.908
CC half 0.982 0.989 0.302
Anomalous completeness 99.7 99.7 98.7
Anomalous multiplicity 3.5 3.5 3.5
Cell 157.928 87.136 87.802 90.0 90.0 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.