X-Ray Diffraction data from PAK4, source of 4FIG structure

Data DOI: 10.15785/SBGRID/434 | ID: 434

Publication DOI: 10.1073/pnas.1214447109

4FIG Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Boggon Laboratory, Yale University School of Medicine

Release Date: March 28, 2017

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/434

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/434 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/434 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/434 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/434 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 434 ; shasum -c files.sha'

Storage requirements: 3.2G

Biological Sample:

PAK4

Dataset Type:

X-Ray Diffraction

Subject Composition:

Protein

Collection Facility:

APS 24-ID-C

Data Creation Date:

June 4, 2011

Related Datasets:

None


Cite this Dataset

Ha, BHak; Boggon, TJ. 2017. "X-Ray Diffraction data for: PAK4. PDB Code 4FIG", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/434.

Download Citation

Dataset Description

X-ray diffraction

Project Members

Name Additional Roles Affiliation While Working on the Project
Titus J BoggonDepositorYale University
Byung Hak HaData CollectorYale University
Titus BoggonPIYale University School of Medicine

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97918

Sweep:

SWEEP1

Files:

/programs/datagrid/434/7P08_1_###.img

Images:

1 - 180

Beam:

(157.43, 156.43) -> (157.43, 156.42)

Distance:

350.0 -> 351.63

Spacegroup:

P 1 21 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 5.04 13.65 5.04
Low resolution limit 71.18 71.19 5.13
Completeness 99.7 100.0 100.0
Multiplicity 3.4 3.1 3.4
I/sigma 11.6 13.9 8.3
Rmerge 0.086 0.063 0.163
CC half 0.985 0.987 0.858
Anomalous completeness 96.4 96.8 97.4
Anomalous multiplicity 1.8 1.8 1.8
Cell 141.998 61.993 142.359 90.0 119.705 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97918

Sweep:

SWEEP1

Files:

/programs/datagrid/434/7P08_1_###.img

Images:

1 - 180

Beam:

(157.43, 156.43) -> (157.43, 156.35)

Distance:

350.0 -> 350.88

Spacegroup:

P 63

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.97 8.05 2.97
Low resolution limit 46.45 46.46 3.02
Completeness 99.9 100.0 100.0
Multiplicity 10.6 9.2 11.3
I/sigma 11.5 33.5 1.0
Rmerge 0.276 0.059 3.099
CC half 0.995 0.997 0.374
Anomalous completeness 99.7 99.7 100.0
Anomalous multiplicity 5.5 5.5 5.5
Cell 141.91 141.91 61.85 90.0 90.0 120.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97918

Sweep:

SWEEP1

Files:

/programs/datagrid/434/7P08_1_###.img

Images:

1 - 180

Beam:

(157.43, 156.43) -> (157.43, 156.35)

Distance:

350.0 -> 351.25

Spacegroup:

P 63

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 4.47 12.07 4.47
Low resolution limit 46.45 46.45 4.55
Completeness 100.0 100.0 100.0
Multiplicity 10.1 7.9 10.4
I/sigma 24.3 32.1 19.8
Rmerge 0.12 0.057 0.259
CC half 0.997 0.997 0.983
Anomalous completeness 100.0 98.4 100.0
Anomalous multiplicity 5.3 5.3 5.3
Cell 141.9 141.9 61.85 90.0 90.0 120.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97918

Sweep:

SWEEP1

Files:

/programs/datagrid/434/7P08_1_###.img

Images:

1 - 180

Beam:

(157.43, 156.43) -> (157.43, 156.33)

Distance:

350.0 -> 337.79

Spacegroup:

P 1 21 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 3.74 10.12 3.74
Low resolution limit 55.03 55.04 3.8
Completeness 72.8 99.8 57.9
Multiplicity 2.5 3.2 3.3
I/sigma 4.9 10.8 3.8
Rmerge 0.253 0.037 0.807
CC half 0.89 0.997 0.323
Anomalous completeness 50.2 94.2 55.3
Anomalous multiplicity 1.5 1.5 1.5
Cell 141.797 61.45 140.595 90.0 119.249 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.