X-Ray Diffraction data from MAPK13 complex with compound 117, source of 5EKO structure

Data DOI: 10.15785/SBGRID/342 | ID: 342

Publication DOI: 10.1016/j.bbagen.2016.06.023

5EKO Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Brett Laboratory, Washington U. School of Medicine

Release Date: Aug. 5, 2016

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/342

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/342 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/342 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/342 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/342 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 342 ; shasum -c files.sha'

Storage requirements: 3.2G

Biological Sample:

MAPK13 complex with compound 117

Dataset Type:

X-Ray Diffraction

Subject Composition:

Ligand, Protein

Collection Facility:

APS 19-ID

Data Creation Date:

Aug. 20, 2011

Related Datasets:

None


Cite this Dataset

Brett, TJ; Brett, T. 2016. "X-Ray Diffraction data for: MAPK13 complex with compound 117. PDB Code 5EKO", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/342.

Download Citation

Dataset Description

Native data set

Project Members

Name Additional Roles Affiliation While Working on the Project
Thomas J BrettData Collector, DepositorWashington University School of Medicine
Tom BrettPIWashington U. School of Medicine

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Reprocessing failed.

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97901

Sweep:

SWEEP1

Files:

/programs/datagrid/342/n117_3.####.img

Images:

1 - 180

Beam:

(154.78, 160.27) -> (154.78, 161.62)

Distance:

292.24 -> 292.74

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.81 4.91 1.81
Low resolution limit 41.23 41.24 1.84
Completeness 88.1 100.0 47.1
Multiplicity 6.9 6.5 5.6
I/sigma 14.9 39.2 0.7
Rmerge 0.089 0.036 2.341
CC half 0.998 0.998 0.161
Anomalous completeness 86.5 99.1 44.1
Anomalous multiplicity 3.7 3.7 3.7
Cell 61.26 69.68 92.96 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97901

Sweep:

SWEEP1

Files:

/programs/datagrid/342/n117_3.####.img

Images:

1 - 180

Beam:

(154.78, 160.27) -> (154.78, 161.62)

Distance:

292.24 -> 292.84

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.83 4.97 1.83
Low resolution limit 46.01 46.02 1.86
Completeness 91.1 100.0 45.1
Multiplicity 6.9 6.5 5.9
I/sigma 14.9 39.3 0.7
Rmerge 0.088 0.036 2.296
CC half 0.998 0.998 -0.15
Anomalous completeness 89.7 99.1 43.3
Anomalous multiplicity 3.7 3.7 3.7
Cell 61.26 69.68 92.96 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97901

Sweep:

SWEEP1

Files:

/programs/datagrid/342/n117_3.####.img

Images:

1 - 180

Beam:

(154.78, 160.27) -> (154.78, 161.6)

Distance:

292.24 -> 292.42

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.82 4.94 1.82
Low resolution limit 55.71 55.73 1.85
Completeness 93.7 100.0 58.6
Multiplicity 6.8 6.5 5.4
I/sigma 8.1 15.3 1.6
Rmerge 0.163 0.083 3.054
CC half 0.972 0.985 0.179
Anomalous completeness 92.5 99.9 54.5
Anomalous multiplicity 3.6 3.6 3.6
Cell 61.2 69.606 92.903 90.0 90.0 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.