X-Ray Diffraction data from Human thrombin-sulfated madanin complex, source of 5L6N structure

Data DOI: 10.15785/SBGRID/324 | ID: 324

Publication DOI: 10.1038/NCHEM.2744

5L6N Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Pereira Laboratory, IBMC/i3S, Universidade do Porto

Release Date: March 24, 2017

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/324

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/324 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/324 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/324 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/324 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 324 ; shasum -c files.sha'

Storage requirements: 16G

Biological Sample:

Human thrombin-sulfated madanin complex

Dataset Type:

X-Ray Diffraction

Subject Composition:

Protein

Collection Facility:

ESRF ID29

Data Creation Date:

March 22, 2017

Related Datasets:

None


Cite this Dataset

Ripoll-Rozada, J; Pereira, PJB. 2017. "X-Ray Diffraction data for: Human thrombin-sulfated madanin complex. PDB Code 5L6N", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/324.

Download Citation

Dataset Description

X-ray Diffraction data from Human thrombin in complex with a disulfated madanin-1 fragment, source of 5L6N structure

Project Members

Name Additional Roles Affiliation While Working on the Project
Pedro JB PereiraData Collector, DepositorIBMC-Instituto de Biologia Molecular e Celular, Universidade do Porto
Jorge Ripoll-RozadaIBMC-Instituto de Biologia Molecular e Celular, Universidade do Porto
Pedro PereiraPIUniversidade do Porto

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Reprocessing failed.

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.96863

Sweep:

SWEEP1

Files:

/programs/datagrid/324/af6556_w1_2_####.cbf

Images:

1 - 2700

Beam:

(215.81, 211.95) -> (215.81, 212.33)

Distance:

300.02 -> 300.31

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.65 4.48 1.65
Low resolution limit 44.55 44.57 1.68
Completeness 99.8 99.4 99.9
Multiplicity 4.9 4.6 5.0
I/sigma 12.7 37.0 1.2
Rmerge 0.05 0.027 1.002
CC half 0.999 0.998 0.468
Anomalous completeness 96.5 94.6 98.1
Anomalous multiplicity 2.6 2.6 2.6
Cell 44.55 80.25 91.39 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.96863

Sweep:

SWEEP1

Files:

/programs/datagrid/324/af6556_w1_2_####.cbf

Images:

1 - 2700

Beam:

(215.81, 211.95) -> (215.81, 212.34)

Distance:

300.02 -> 299.95

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.65 4.48 1.65
Low resolution limit 44.55 44.57 1.68
Completeness 99.7 99.3 99.9
Multiplicity 4.9 4.6 5.0
I/sigma 12.7 37.5 1.2
Rmerge 0.049 0.026 1.001
CC half 0.999 0.999 0.467
Anomalous completeness 96.4 94.4 98.1
Anomalous multiplicity 2.6 2.6 2.6
Cell 44.55 80.25 91.39 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.96863

Sweep:

SWEEP1

Files:

/programs/datagrid/324/af6556_w1_2_####.cbf

Images:

1 - 2700

Beam:

(215.81, 211.95) -> (215.81, 212.31)

Distance:

300.02 -> 299.95

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.58 4.29 1.58
Low resolution limit 44.51 44.53 1.61
Completeness 99.8 99.9 99.2
Multiplicity 4.8 4.7 4.9
I/sigma 10.0 31.5 1.1
Rmerge 0.061 0.032 1.066
CC half 0.999 0.998 0.499
Anomalous completeness 97.1 97.0 97.2
Anomalous multiplicity 2.5 2.5 2.5
Cell 44.514 80.173 91.33 90.0 90.0 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.