X-Ray Diffraction data from Crystal structure of a LonA protease domain in complex with bortezomib, source of 4YPM structure

Data DOI: 10.15785/SBGRID/314 | ID: 314

Publication DOI: 10.1016/j.str.2016.03.003

4YPM Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Chang Laboratory, Academia Sinica

Release Date: May 31, 2016

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/314

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/314 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/314 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/314 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/314 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 314 ; shasum -c files.sha'

Storage requirements: 12G

Biological Sample:

Crystal structure of a LonA protease domain in complex with bortezomib

Dataset Type:

X-Ray Diffraction

Subject Composition:

Ligand, Protein

Collection Facility:

BL15A, NSRRC

Data Creation Date:

March 18, 2014

Related Datasets:

None


Cite this Dataset

Su, M; Lin, C; Chang, C. 2016. "X-Ray Diffraction data for: Crystal structure of a LonA protease domain in complex with bortezomib. PDB Code 4YPM", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/314.

Download Citation

Dataset Description

Native dataset

Project Members

Name Additional Roles Affiliation While Working on the Project
Ming-Yuan SuDepositorAcademia Sinica
Chien-Chu LinData CollectorAcademia Sinica
Chung-I ChangPIAcademia Sinica

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.0

Sweep:

SWEEP1

Files:

/programs/datagrid/314/MtAAAP_bortezomib_7_3_11_###.mccd

Images:

1 - 360

Beam:

(150.0, 150.0) -> (150.0, 150.17)

Distance:

220.0 -> 219.83

Spacegroup:

P 6 2 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.57 4.26 1.57
Low resolution limit 52.94 52.97 1.6
Completeness 100.0 100.0 99.3
Multiplicity 19.9 20.0 10.6
I/sigma 13.4 40.0 1.6
Rmerge 0.153 0.044 1.351
CC half 0.999 0.998 0.33
Anomalous completeness 100.0 100.0 99.6
Anomalous multiplicity 10.5 10.5 10.5
Cell 122.256 122.256 103.008 90.0 90.0 120.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.0

Sweep:

SWEEP1

Files:

/programs/datagrid/314/MtAAAP_bortezomib_7_3_11_###.mccd

Images:

1 - 360

Beam:

(150.0, 150.0) -> (150.0, 150.05)

Distance:

220.0 -> 219.75

Spacegroup:

P 6 2 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.6 4.34 1.6
Low resolution limit 25.04 25.05 1.63
Completeness 99.9 99.8 99.8
Multiplicity 20.7 19.3 12.6
I/sigma 19.8 76.3 1.1
Rmerge 0.12 0.027 2.123
CC half 0.999 1.0 0.421
Anomalous completeness 100.0 99.9 99.8
Anomalous multiplicity 10.9 10.9 10.9
Cell 122.34 122.34 103.1 90.0 90.0 120.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.0

Sweep:

SWEEP1

Files:

/programs/datagrid/314/MtAAAP_bortezomib_7_3_11_###.mccd

Images:

1 - 360

Beam:

(150.0, 150.0) -> (150.0, 150.05)

Distance:

220.0 -> 219.83

Spacegroup:

P 6 2 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.58 4.28 1.58
Low resolution limit 26.49 26.49 1.61
Completeness 99.9 99.8 99.5
Multiplicity 20.3 19.4 11.4
I/sigma 19.1 76.3 0.9
Rmerge 0.122 0.027 2.328
CC half 0.999 1.0 0.365
Anomalous completeness 100.0 99.9 99.6
Anomalous multiplicity 10.7 10.7 10.7
Cell 122.34 122.34 103.1 90.0 90.0 120.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.0

Sweep:

SWEEP1

Files:

/programs/datagrid/314/MtAAAP_bortezomib_7_3_11_###.mccd

Images:

1 - 360

Beam:

(150.0, 150.0) -> (150.0, 150.14)

Distance:

220.0 -> 220.0

Spacegroup:

P 6 2 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.57 4.26 1.57
Low resolution limit 37.38 37.39 1.6
Completeness 99.9 100.0 98.9
Multiplicity 20.0 20.1 10.3
I/sigma 14.0 41.4 1.0
Rmerge 0.136 0.038 2.421
CC half 0.998 0.998 0.471
Anomalous completeness 100.0 100.0 99.2
Anomalous multiplicity 10.6 10.6 10.6
Cell 122.506 122.506 103.25 90.0 90.0 120.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.