Data DOI: 10.15785/SBGRID/283 | ID: 283
Publication DOI: 10.1107/S2053230X15015939
4YBO Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB
Kappock Laboratory, Purdue University
Release Date: May 27, 2016
1. If this dataset is locally available, it should be accessable at /programs/datagrid/283
2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:
'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/283 .' (Harvard Medical School, USA)
Depending on your location, faster access may be available from a Tier 1 site closer to your location
'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/283 .' (Uppsala University, Sweden)
'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/283 .' (Institut Pasteur de Montevideo, Uruguay)
'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/283 .' (Shanghai Institutes for Biological Sciences, China)
3. After the transfer is completed, please issue the following command to verify data integrity:
'cd 283 ; shasum -c files.sha'
Storage requirements: 25G
Biological Sample:
citrate synthase (TpCS) with C-terminal His6 tag
Dataset Type:
X-Ray Diffraction
Subject Composition:
Protein
Collection Facility:
beamline 21-ID-G, LS-CAT, APS, Chicago, IL
Data Creation Date:
July 2, 2010
Related Datasets:
None
Donini, S; Kappock, T. 2016. "X-Ray Diffraction data for: citrate synthase (TpCS) with C-terminal His6 tag. PDB Code 4YBO", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/283.
Structure of citrate synthase from the thermoacidophilic euryarchaeon Thermolasma acidophilum
| Name | Additional Roles | Affiliation While Working on the Project |
|---|---|---|
| Stefano Donini | Data Collector | Purdue University |
| T. Joseph Kappock | Depositor, PI | Purdue University |
none
Version:
version unreported
Reprocessing failed.
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 0.97856
Sweep:
SWEEP3
Files:
/programs/datagrid/283/TpCS_v3.###
Images:
1 - 360
Beam:
(153.72, 147.99) -> (153.72, 147.93)
Distance:
250.0 -> 247.64
Spacegroup:
P 1 21 1
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 1.87 | 5.07 | 1.87 |
| Low resolution limit | 39.85 | 39.86 | 1.9 |
| Completeness | 97.7 | 99.3 | 96.3 |
| Multiplicity | 14.0 | 14.2 | 5.0 |
| I/sigma | 10.6 | 33.0 | 0.8 |
| Rmerge | 0.208 | 0.062 | 1.667 |
| CC half | 0.996 | 0.998 | 0.455 |
| Anomalous completeness | 97.7 | 99.5 | 95.2 |
| Anomalous multiplicity | 7.1 | 7.1 | 7.1 |
| Cell | 56.42 | 113.23 | 120.02 | 90.0 | 95.08 | 90.0 |
|---|
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 0.97856
Sweep:
SWEEP3
Files:
/programs/datagrid/283/TpCS_v3.###
Images:
1 - 360
Beam:
(153.72, 147.99) -> (153.72, 147.91)
Distance:
250.0 -> 249.64
Spacegroup:
P 1 21 1
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 1.89 | 5.13 | 1.89 |
| Low resolution limit | 40.14 | 40.15 | 1.92 |
| Completeness | 97.8 | 99.5 | 96.1 |
| Multiplicity | 13.7 | 14.1 | 4.9 |
| I/sigma | 10.7 | 33.0 | 0.9 |
| Rmerge | 0.204 | 0.06 | 1.454 |
| CC half | 0.997 | 0.998 | 0.525 |
| Anomalous completeness | 97.6 | 99.6 | 95.4 |
| Anomalous multiplicity | 6.9 | 6.9 | 6.9 |
| Cell | 56.48 | 113.33 | 120.07 | 90.0 | 95.11 | 90.0 |
|---|
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 0.97856
Sweep:
SWEEP3
Files:
/programs/datagrid/283/TpCS_v3.###
Images:
1 - 360
Beam:
(153.72, 147.99) -> (153.72, 148.01)
Distance:
250.0 -> 250.16
Spacegroup:
P 1 21 1
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 2.0 | 5.42 | 2.0 |
| Low resolution limit | 32.39 | 32.4 | 2.03 |
| Completeness | 97.8 | 99.0 | 92.2 |
| Multiplicity | 13.7 | 14.0 | 4.8 |
| I/sigma | 4.7 | 9.3 | 0.9 |
| Rmerge | 0.533 | 0.206 | 11.622 |
| CC half | 0.959 | 0.981 | 0.25 |
| Anomalous completeness | 97.3 | 99.3 | 86.7 |
| Anomalous multiplicity | 6.9 | 6.9 | 6.9 |
| Cell | 56.268 | 112.768 | 119.657 | 90.0 | 94.933 | 90.0 |
|---|
License: CC0
Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.
