X-Ray Diffraction data from succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18) bound to CoA and citrate, source of 4EUD structure

Data DOI: 10.15785/SBGRID/281 | ID: 281

Publication DOI: 10.1021/bi300957f

4EUD Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Kappock Laboratory, Purdue University

Release Date: May 27, 2016

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/281

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/281 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/281 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/281 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/281 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 281 ; shasum -c files.sha'

Storage requirements: 12G

Biological Sample:

succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18) bound to CoA and citrate

Dataset Type:

X-Ray Diffraction

Subject Composition:

Ligand, Protein

Collection Facility:

beamline 23-ID-B, GM/CA, APS, Chicago, IL

Data Creation Date:

July 2, 2010

Related Datasets:

None


Cite this Dataset

Mullins, EA.; Kappock, T. 2016. "X-Ray Diffraction data for: succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18) bound to CoA and citrate. PDB Code 4EUD", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/281.

Download Citation

Dataset Description

Succinyl-CoA:acetate CoA-transferase (AarC) in complex with CoA and citrate

Project Members

Name Additional Roles Affiliation While Working on the Project
Elwood A. MullinsData CollectorPurdue University
T. Joseph KappockDepositor, PIPurdue University

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.0332

Sweep:

SWEEP1

Files:

/programs/datagrid/281/aarc_70_1.####

Images:

1 - 360

Beam:

(150.0, 150.0) -> (150.0, 150.32)

Distance:

250.0 -> 251.12

Spacegroup:

P 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.15 5.83 2.15
Low resolution limit 67.81 67.84 2.19
Completeness 96.5 98.6 94.4
Multiplicity 3.9 4.0 3.8
I/sigma 5.7 9.7 3.0
Rmerge 0.313 0.083 0.958
CC half 0.885 0.968 0.281
Anomalous completeness 94.6 98.2 90.4
Anomalous multiplicity 1.9 1.9 1.9
Cell 67.806 111.023 119.951 90.244 90.006 90.152

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.0332

Sweep:

SWEEP1

Files:

/programs/datagrid/281/aarc_70_1.####

Images:

1 - 360

Beam:

(150.0, 150.0) -> (150.0, 150.2)

Distance:

250.0 -> 249.38

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.86 5.05 1.86
Low resolution limit 52.54 52.56 1.89
Completeness 99.0 100.0 87.0
Multiplicity 13.9 13.1 11.4
I/sigma 8.9 26.5 1.0
Rmerge 0.406 0.086 2.458
CC half 0.987 0.996 0.412
Anomalous completeness 98.9 99.9 87.1
Anomalous multiplicity 7.2 7.2 7.2
Cell 67.64 110.3 119.52 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.0332

Sweep:

SWEEP1

Files:

/programs/datagrid/281/aarc_70_1.####

Images:

1 - 360

Beam:

(150.0, 150.0) -> (150.0, 150.21)

Distance:

250.0 -> 250.56

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.87 5.07 1.87
Low resolution limit 57.65 57.68 1.9
Completeness 99.3 100.0 88.6
Multiplicity 13.9 13.0 11.7
I/sigma 9.1 26.5 1.1
Rmerge 0.4 0.085 2.264
CC half 0.987 0.996 0.416
Anomalous completeness 99.1 100.0 88.7
Anomalous multiplicity 7.3 7.3 7.3
Cell 67.63 110.29 119.51 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.0332

Sweep:

SWEEP1

Files:

/programs/datagrid/281/aarc_70_1.####

Images:

1 - 360

Beam:

(150.0, 150.0) -> (150.0, 150.29)

Distance:

250.0 -> 244.5

Spacegroup:

P 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.33 6.32 2.33
Low resolution limit 80.06 80.1 2.37
Completeness 97.3 99.6 74.7
Multiplicity 4.0 4.0 3.9
I/sigma 5.3 8.2 3.2
Rmerge 0.36 0.083 2.163
CC half 0.885 0.978 0.269
Anomalous completeness 97.1 99.4 74.3
Anomalous multiplicity 2.0 2.0 2.0
Cell 66.655 108.596 118.148 89.852 89.891 89.933

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.