X-Ray Diffraction data from succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18) bound to CoA and citrate, source of 4EUD structure

Data DOI: 10.15785/SBGRID/281 | ID: 281

Publication DOI: 10.1021/bi300957f

4EUD Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Kappock Laboratory, Purdue University

Release Date: May 27, 2016

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/281

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/281 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/281 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/281 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/281 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 281 ; shasum -c files.sha'

Storage requirements: 12G

Biological Sample:

succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18) bound to CoA and citrate

Dataset Type:

X-Ray Diffraction

Subject Composition:

Ligand, Protein

Collection Facility:

beamline 23-ID-B, GM/CA, APS, Chicago, IL

Data Creation Date:

July 2, 2010

Related Datasets:

None


Cite this Dataset

Mullins, EA.; Kappock, T. 2016. "X-Ray Diffraction data for: succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18) bound to CoA and citrate. PDB Code 4EUD", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/281.

Download Citation

Dataset Description

Succinyl-CoA:acetate CoA-transferase (AarC) in complex with CoA and citrate

Project Members

Name Additional Roles Affiliation While Working on the Project
Elwood A. MullinsData CollectorPurdue University
T. Joseph KappockDepositor, PIPurdue University

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.0332

Sweep:

SWEEP1

Files:

/programs/datagrid/281/aarc_70_1.####

Images:

1 - 360

Beam:

(150.0, 150.0) -> (150.0, 150.2)

Distance:

250.0 -> 249.41

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.78 4.83 1.78
Low resolution limit 50.07 50.09 1.81
Completeness 96.3 100.0 70.3
Multiplicity 13.5 12.8 10.1
I/sigma 9.1 26.5 0.8
Rmerge 0.586 0.086 4.631
CC half 0.98 0.995 0.281
Anomalous completeness 96.0 99.6 70.1
Anomalous multiplicity 7.0 7.0 7.0
Cell 67.62 110.28 119.49 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.0332

Sweep:

SWEEP1

Files:

/programs/datagrid/281/aarc_70_1.####

Images:

1 - 360

Beam:

(150.0, 150.0) -> (150.0, 150.21)

Distance:

250.0 -> 250.56

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.78 4.83 1.78
Low resolution limit 55.11 55.14 1.81
Completeness 96.3 100.0 70.7
Multiplicity 13.5 12.8 10.1
I/sigma 9.1 26.5 0.8
Rmerge 0.577 0.086 4.707
CC half 0.98 0.996 0.279
Anomalous completeness 96.0 99.6 70.6
Anomalous multiplicity 7.0 7.0 7.0
Cell 67.58 110.22 119.45 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.0332

Sweep:

SWEEP1

Files:

/programs/datagrid/281/aarc_70_1.####

Images:

1 - 360

Beam:

(150.0, 150.0) -> (150.0, 150.29)

Distance:

250.0 -> 243.35

Spacegroup:

P 2 21 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.53 4.16 1.53
Low resolution limit 108.72 109.0 1.56
Completeness 76.4 100.0 16.1
Multiplicity 11.9 14.2 6.6
I/sigma 12.7 13.4 20.4
Rmerge 0.273 0.433 0.184
CC half 0.921 0.974 0.003
Anomalous completeness 75.7 100.0 15.4
Anomalous multiplicity 6.2 6.2 6.2
Cell 66.682 108.723 118.235 90.0 90.0 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.