X-Ray Diffraction data from succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18), S71A mutant, source of 4EU8 structure

Data DOI: 10.15785/SBGRID/276 | ID: 276

Publication DOI: 10.1021/bi300957f

4EU8 Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Kappock Laboratory, Purdue University

Release Date: May 27, 2016

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/276

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/276 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/276 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/276 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/276 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 276 ; shasum -c files.sha'

Storage requirements: 6.4G

Biological Sample:

succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18), S71A mutant

Dataset Type:

X-Ray Diffraction

Subject Composition:

Ligand, Protein

Collection Facility:

beamline 21-ID-F, LS-CAT, APS, Chicago, IL

Data Creation Date:

July 23, 2011

Related Datasets:

None


Cite this Dataset

Mullins, EA.; Kappock, T. 2016. "X-Ray Diffraction data for: succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18), S71A mutant. PDB Code 4EU8", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/276.

Download Citation

Dataset Description

Succinyl-CoA:acetate CoA-transferase (AarCH6-S71A) in complex with CoA

Project Members

Name Additional Roles Affiliation While Working on the Project
Elwood A. MullinsData CollectorPurdue University
T. Joseph KappockDepositor, PIPurdue University

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97872

Sweep:

SWEEP1

Files:

/programs/datagrid/276/aarch6_110.###

Images:

1 - 360

Beam:

(111.39, 111.97) -> (111.39, 111.98)

Distance:

180.0 -> 180.22

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.51 4.1 1.51
Low resolution limit 58.64 58.68 1.54
Completeness 90.4 100.0 50.5
Multiplicity 12.9 14.2 6.3
I/sigma 11.4 26.4 1.2
Rmerge 0.142 0.084 1.576
CC half 0.997 0.996 0.226
Anomalous completeness 90.3 99.8 50.6
Anomalous multiplicity 6.7 6.7 6.7
Cell 67.225 109.638 119.924 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97872

Sweep:

SWEEP1

Files:

/programs/datagrid/276/aarch6_110.###

Images:

1 - 360

Beam:

(111.39, 111.97) -> (111.39, 111.89)

Distance:

180.0 -> 180.01

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.54 4.18 1.54
Low resolution limit 49.86 49.89 1.57
Completeness 93.1 100.0 59.5
Multiplicity 13.0 13.2 7.0
I/sigma 15.7 44.1 1.1
Rmerge 0.101 0.046 1.542
CC half 0.999 0.998 0.386
Anomalous completeness 93.0 100.0 59.2
Anomalous multiplicity 6.7 6.7 6.7
Cell 67.22 109.63 120.03 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97872

Sweep:

SWEEP1

Files:

/programs/datagrid/276/aarch6_110.###

Images:

1 - 360

Beam:

(111.39, 111.97) -> (111.39, 111.88)

Distance:

180.0 -> 180.07

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.54 4.18 1.54
Low resolution limit 60.01 60.06 1.57
Completeness 93.1 100.0 59.5
Multiplicity 13.0 13.2 7.0
I/sigma 15.7 44.0 1.1
Rmerge 0.101 0.046 1.541
CC half 0.999 0.998 0.395
Anomalous completeness 93.0 100.0 59.2
Anomalous multiplicity 6.7 6.7 6.7
Cell 67.22 109.63 120.03 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97872

Sweep:

SWEEP1

Files:

/programs/datagrid/276/aarch6_110.###

Images:

1 - 360

Beam:

(111.39, 111.97) -> (111.39, 111.94)

Distance:

180.0 -> 179.96

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.53 4.15 1.53
Low resolution limit 59.99 60.04 1.56
Completeness 91.9 100.0 55.2
Multiplicity 13.0 14.2 6.7
I/sigma 11.2 26.5 1.1
Rmerge 0.133 0.074 2.107
CC half 0.998 0.997 0.433
Anomalous completeness 91.8 100.0 55.3
Anomalous multiplicity 6.8 6.8 6.8
Cell 67.233 109.549 119.986 90.0 90.0 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.