X-Ray Diffraction data from succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18) bound to CoA and citrate, source of 4EU7 structure

Data DOI: 10.15785/SBGRID/275 | ID: 275

Publication DOI: 10.1021/bi300957f

4EU7 Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Kappock Laboratory, Purdue University

Release Date: May 27, 2016

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/275

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/275 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/275 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/275 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/275 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 275 ; shasum -c files.sha'

Storage requirements: 12G

Biological Sample:

succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18) bound to CoA and citrate

Dataset Type:

X-Ray Diffraction

Subject Composition:

Ligand, Protein

Collection Facility:

beamline 21-ID-G, LS-CAT, APS, Chicago, IL

Data Creation Date:

Dec. 9, 2009

Related Datasets:

None


Cite this Dataset

Mullins, EA.; Kappock, T. 2016. "X-Ray Diffraction data for: succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18) bound to CoA and citrate. PDB Code 4EU7", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/275.

Download Citation

Dataset Description

Succinyl-CoA:acetate CoA-transferase (AarCH6) in complex with CoA and citrate

Project Members

Name Additional Roles Affiliation While Working on the Project
Elwood A. MullinsData CollectorPurdue University
T. Joseph KappockDepositor, PIPurdue University

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/275/aarch6_36i.###

Images:

1 - 360

Beam:

(153.83, 148.07) -> (153.83, 148.07)

Distance:

200.0 -> 200.06

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.47 3.99 1.47
Low resolution limit 58.79 58.84 1.5
Completeness 99.9 100.0 97.8
Multiplicity 14.1 14.3 8.9
I/sigma 11.5 36.9 1.1
Rmerge 0.18 0.047 1.967
CC half 0.998 0.999 0.241
Anomalous completeness 99.8 100.0 97.5
Anomalous multiplicity 7.3 7.3 7.3
Cell 67.388 110.718 120.272 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/275/aarch6_36i.###

Images:

1 - 360

Beam:

(153.83, 148.07) -> (153.83, 147.95)

Distance:

200.0 -> 199.86

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.5 4.07 1.5
Low resolution limit 34.87 34.88 1.53
Completeness 100.0 100.0 99.5
Multiplicity 14.5 14.1 10.9
I/sigma 14.7 52.4 1.1
Rmerge 0.145 0.04 2.039
CC half 0.999 0.999 0.423
Anomalous completeness 99.9 99.9 99.2
Anomalous multiplicity 7.5 7.5 7.5
Cell 67.38 110.81 120.33 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/275/aarch6_36i.###

Images:

1 - 360

Beam:

(153.83, 148.07) -> (153.83, 147.95)

Distance:

200.0 -> 199.98

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.49 4.04 1.49
Low resolution limit 35.31 35.32 1.52
Completeness 100.0 100.0 99.3
Multiplicity 14.4 14.1 10.1
I/sigma 14.4 52.3 1.0
Rmerge 0.147 0.04 2.115
CC half 0.999 0.999 0.383
Anomalous completeness 99.9 99.9 99.0
Anomalous multiplicity 7.4 7.4 7.4
Cell 67.38 110.81 120.33 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/275/aarch6_36i.###

Images:

1 - 360

Beam:

(153.83, 148.07) -> (153.83, 148.03)

Distance:

200.0 -> 200.03

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.51 4.1 1.51
Low resolution limit 42.8 42.82 1.54
Completeness 99.9 100.0 97.5
Multiplicity 14.1 14.3 9.0
I/sigma 12.3 37.9 1.2
Rmerge 0.148 0.042 3.098
CC half 0.999 0.999 0.518
Anomalous completeness 99.8 100.0 96.9
Anomalous multiplicity 7.3 7.3 7.3
Cell 67.37 110.861 120.328 90.0 90.0 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.