Data DOI: 10.15785/SBGRID/274 | ID: 274
Publication DOI: 10.1021/bi300957f
4EU6 Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB
Kappock Laboratory, Purdue University
Release Date: 27 May 2016
1. If this dataset is locally available, it should be accessable at /programs/datagrid/274
2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:
'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/274 .' (Harvard Medical School, USA)
Depending on your location, faster access may be available from a Tier 1 site closer to your location
'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/274 .' (Uppsala University, Sweden)
'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/274 .' (Institut Pasteur de Montevideo, Uruguay)
'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/274 .' (Shanghai Institutes for Biological Sciences, China)
3. After the transfer is completed, please issue the following command to verify data integrity:
'cd 274 ; shasum -c files.sha'
Storage requirements: 6.4G
Biological Sample:
succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18) with covalent adducts
Dataset Type:
X-Ray Diffraction
Subject Composition:
Ligand, Protein
Collection Facility:
beamline 21-ID-F, LS-CAT, APS, Chicago, IL
Data Creation Date:
23 Jul 2011
Related Datasets:
None
Mullins, EA.; Kappock, T. 2016. "X-Ray Diffraction data for: succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18) with covalent adducts. PDB Code 4EU6", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/274.
Succinyl-CoA:acetate CoA-transferase (AarCH6) in complex with CoA, acetate, and covalent acetylglutamyl anhydride and glutamyl-CoA thioester adducts
| Name | Additional Roles | Affiliation While Working on the Project |
|---|---|---|
| Elwood A. Mullins | Data Collector | Purdue University |
| T. Joseph Kappock | Depositor, PI | Purdue University |
none
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 0.97872
Sweep:
SWEEP1
Files:
/programs/datagrid/274/aarch6_101.###
Images:
1 - 360
Beam:
(111.41, 112.02) -> (111.41, 111.93)
Distance:
155.0 -> 155.46
Spacegroup:
P 21 21 21
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 1.51 | 4.1 | 1.51 |
| Low resolution limit | 50.21 | 50.24 | 1.54 |
| Completeness | 100.0 | 100.0 | 98.6 |
| Multiplicity | 14.0 | 13.7 | 8.8 |
| I/sigma | 12.7 | 46.4 | 0.8 |
| Rmerge | 0.178 | 0.041 | 2.694 |
| CC half | 0.999 | 0.999 | 0.295 |
| Anomalous completeness | 99.9 | 100.0 | 98.7 |
| Anomalous multiplicity | 7.3 | 7.3 | 7.3 |
| Cell | 67.19 | 110.59 | 119.88 | 90.0 | 90.0 | 90.0 |
|---|
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 0.97872
Sweep:
SWEEP1
Files:
/programs/datagrid/274/aarch6_101.###
Images:
1 - 360
Beam:
(111.41, 112.02) -> (111.41, 111.93)
Distance:
155.0 -> 155.39
Spacegroup:
P 21 21 21
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 1.51 | 4.1 | 1.51 |
| Low resolution limit | 59.94 | 59.99 | 1.54 |
| Completeness | 100.0 | 100.0 | 98.6 |
| Multiplicity | 14.0 | 13.7 | 8.8 |
| I/sigma | 12.7 | 46.4 | 0.8 |
| Rmerge | 0.178 | 0.041 | 2.691 |
| CC half | 0.999 | 0.999 | 0.295 |
| Anomalous completeness | 99.9 | 99.9 | 98.7 |
| Anomalous multiplicity | 7.3 | 7.3 | 7.3 |
| Cell | 67.19 | 110.59 | 119.88 | 90.0 | 90.0 | 90.0 |
|---|
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 0.97872
Sweep:
SWEEP1
Files:
/programs/datagrid/274/aarch6_101.###
Images:
1 - 360
Beam:
(111.41, 112.02) -> (111.41, 111.99)
Distance:
155.0 -> 155.52
Spacegroup:
P 21 21 21
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 1.41 | 3.83 | 1.41 |
| Low resolution limit | 59.98 | 60.03 | 1.44 |
| Completeness | 97.8 | 100.0 | 77.9 |
| Multiplicity | 12.9 | 14.5 | 5.7 |
| I/sigma | 5.2 | 36.8 | 1.4 |
| Rmerge | 0.345 | 0.058 | 1.509 |
| CC half | 0.578 | 0.998 | 0.468 |
| Anomalous completeness | 97.8 | 100.0 | 78.5 |
| Anomalous multiplicity | 6.7 | 6.7 | 6.7 |
| Cell | 67.239 | 110.775 | 119.954 | 90.0 | 90.0 | 90.0 |
|---|
License: CC0
Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.
