X-Ray Diffraction data from succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18), source of 4EU4 structure

Data DOI: 10.15785/SBGRID/271 | ID: 271

Publication DOI: 10.1021/bi300957f

4EU4 Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Kappock Laboratory, Purdue University

Release Date: May 27, 2016

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/271

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/271 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/271 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/271 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/271 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 271 ; shasum -c files.sha'

Storage requirements: 13G

Biological Sample:

succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18)

Dataset Type:

X-Ray Diffraction

Subject Composition:

Ligand, Protein

Collection Facility:

beamline 21-ID-G, LS-CAT, APS, Chicago, IL

Data Creation Date:

Oct. 9, 2009

Related Datasets:

None


Cite this Dataset

Mullins, EA.; Kappock, T. 2016. "X-Ray Diffraction data for: succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18). PDB Code 4EU4", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/271.

Download Citation

Dataset Description

Succinyl-CoA:acetate CoA-transferase (AarCH6) in complex with CoA (hexagonal lattice)

Project Members

Name Additional Roles Affiliation While Working on the Project
Elwood A. MullinsData CollectorPurdue University
T. Joseph KappockDepositor, PIPurdue University

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/271/aarch6_15d.###

Images:

1 - 400

Beam:

(154.04, 147.8) -> (154.04, 147.81)

Distance:

375.0 -> 374.91

Spacegroup:

P 62 2 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.41 6.54 2.41
Low resolution limit 118.43 118.57 2.45
Completeness 93.3 100.0 77.8
Multiplicity 20.9 22.0 14.9
I/sigma 13.6 34.3 1.2
Rmerge 0.213 0.052 2.695
CC half 0.997 0.998 0.353
Anomalous completeness 92.6 100.0 78.3
Anomalous multiplicity 11.2 11.2 11.2
Cell 149.799 149.799 290.146 90.0 90.0 120.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/271/aarch6_15d.###

Images:

1 - 400

Beam:

(154.04, 147.8) -> (154.04, 147.69)

Distance:

375.0 -> 374.47

Spacegroup:

P 62 2 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.47 6.69 2.47
Low resolution limit 34.98 34.98 2.51
Completeness 100.0 100.0 97.9
Multiplicity 23.4 21.3 17.4
I/sigma 19.8 59.6 1.2
Rmerge 0.145 0.035 2.584
CC half 0.999 0.999 0.453
Anomalous completeness 99.9 99.9 98.6
Anomalous multiplicity 12.5 12.5 12.5
Cell 150.04 150.04 290.21 90.0 90.0 120.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/271/aarch6_15d.###

Images:

1 - 400

Beam:

(154.04, 147.8) -> (154.04, 147.69)

Distance:

375.0 -> 374.46

Spacegroup:

P 62 2 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 2.48 6.72 2.48
Low resolution limit 39.53 39.54 2.52
Completeness 100.0 100.0 98.4
Multiplicity 23.5 21.3 17.9
I/sigma 20.1 59.5 1.2
Rmerge 0.144 0.035 2.52
CC half 0.999 0.999 0.499
Anomalous completeness 99.9 99.9 99.0
Anomalous multiplicity 12.5 12.5 12.5
Cell 150.04 150.04 290.21 90.0 90.0 120.0

Version:

version unreported

Reprocessing failed.


License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.