X-Ray Diffraction data from succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18), partial citrate complex, source of 4EU3 structure

Data DOI: 10.15785/SBGRID/267 | ID: 267

Publication DOI: 10.1021/bi300957f

4EU3 Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Kappock Laboratory, Purdue University

Release Date: May 27, 2016

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/267

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/267 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/267 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/267 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/267 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 267 ; shasum -c files.sha'

Storage requirements: 6.4G

Biological Sample:

succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18), partial citrate complex

Dataset Type:

X-Ray Diffraction

Subject Composition:

Ligand, Protein

Collection Facility:

beamline 21-ID-F, LS-CAT, APS, Chicago, IL

Data Creation Date:

March 15, 2010

Related Datasets:

None


Cite this Dataset

Mullins, EA.; Kappock, T. 2016. "X-Ray Diffraction data for: succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18), partial citrate complex. PDB Code 4EU3", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/267.

Download Citation

Dataset Description

succinyl-CoA:acetate CoA-transferase (AarCH6) in complex with citrate (subunit B) or unliganded (subunit A)

Project Members

Name Additional Roles Affiliation While Working on the Project
Elwood A. MullinsData Collector, DepositorPurdue University
T. Joseph Kappock, PIPurdue University

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97872

Sweep:

SWEEP1

Files:

/programs/datagrid/267/aarch6_48.###

Images:

1 - 360

Beam:

(111.36, 111.91) -> (111.36, 112.11)

Distance:

150.0 -> 149.9

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.38 3.75 1.38
Low resolution limit 44.79 44.81 1.4
Completeness 94.1 100.0 60.8
Multiplicity 13.1 14.4 7.4
I/sigma 13.0 44.4 1.2
Rmerge 0.155 0.047 1.785
CC half 0.998 0.999 0.353
Anomalous completeness 93.6 100.0 59.6
Anomalous multiplicity 6.8 6.8 6.8
Cell 67.438 110.36 119.806 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97872

Sweep:

SWEEP1

Files:

/programs/datagrid/267/aarch6_48.###

Images:

1 - 360

Beam:

(111.36, 111.91) -> (111.36, 112.02)

Distance:

150.0 -> 149.76

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.38 3.74 1.38
Low resolution limit 34.76 34.77 1.4
Completeness 94.5 100.0 62.4
Multiplicity 13.6 14.3 8.0
I/sigma 15.7 62.4 1.1
Rmerge 0.13 0.031 1.796
CC half 0.999 1.0 0.427
Anomalous completeness 94.5 100.0 62.8
Anomalous multiplicity 7.0 7.0 7.0
Cell 67.45 110.28 119.79 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97872

Sweep:

SWEEP1

Files:

/programs/datagrid/267/aarch6_48.###

Images:

1 - 360

Beam:

(111.36, 111.91) -> (111.36, 112.01)

Distance:

150.0 -> 149.84

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.38 3.75 1.38
Low resolution limit 58.77 58.83 1.4
Completeness 94.5 100.0 62.4
Multiplicity 13.5 14.3 8.0
I/sigma 15.7 62.3 1.1
Rmerge 0.13 0.031 1.797
CC half 0.999 1.0 0.427
Anomalous completeness 94.5 100.0 62.8
Anomalous multiplicity 7.0 7.0 7.0
Cell 67.45 110.28 119.79 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97872

Sweep:

SWEEP1

Files:

/programs/datagrid/267/aarch6_48.###

Images:

1 - 360

Beam:

(111.36, 111.91) -> (111.36, 112.08)

Distance:

150.0 -> 149.89

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.38 3.75 1.38
Low resolution limit 57.58 57.63 1.4
Completeness 94.2 100.0 60.2
Multiplicity 13.2 14.5 5.8
I/sigma 14.4 54.8 1.0
Rmerge 0.127 0.033 1.936
CC half 0.999 1.0 0.499
Anomalous completeness 94.0 100.0 58.5
Anomalous multiplicity 6.8 6.8 6.8
Cell 67.488 110.382 119.825 90.0 90.0 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.