X-Ray Diffraction data from BAZ2B bromodomain in complex with fragment F60, source of 5E9I structure

Data DOI: 10.15785/SBGRID/260 | ID: 260

Publication DOI: 10.1021/acschembio.5b00914

5E9I Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Caflisch Laboratory, University of Zurich

Release Date: April 22, 2016

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/260

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/260 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/260 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/260 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/260 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 260 ; shasum -c files.sha'

Storage requirements: 431M

Biological Sample:

BAZ2B bromodomain in complex with fragment F60

Dataset Type:

X-Ray Diffraction

Subject Composition:

Ligand, Protein

Collection Facility:

beamline XRD1, Elettra, Trieste, Italy

Data Creation Date:

May 5, 2015

Related Datasets:

None


Cite this Dataset

Lolli, G; Caflisch, A. 2016. "X-Ray Diffraction data for: BAZ2B bromodomain in complex with fragment F60. PDB Code 5E9I", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/260.

Download Citation

Dataset Description

Native dataset

Project Members

Name Additional Roles Affiliation While Working on the Project
Graziano LolliData Collector, DepositorUniversity of Zurich
Amedeo Caflisch, PIUniversity of Zurich

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.915

Sweep:

SWEEP1

Files:

/programs/datagrid/260/b3s10_2_#####.cbf

Images:

1 - 180

Beam:

(141.56, 126.94) -> (141.56, 126.87)

Distance:

195.0 -> 195.36

Spacegroup:

C 2 2 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.67 4.53 1.67
Low resolution limit 48.05 48.07 1.7
Completeness 99.7 100.0 99.6
Multiplicity 5.6 5.9 5.8
I/sigma 10.1 28.6 1.0
Rmerge 0.076 0.03 1.008
CC half 0.991 0.982 0.73
Anomalous completeness 98.4 98.8 98.9
Anomalous multiplicity 3.0 3.0 3.0
Cell 83.193 96.106 57.929 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.915

Sweep:

SWEEP1

Files:

/programs/datagrid/260/b3s10_2_#####.cbf

Images:

1 - 180

Beam:

(141.56, 126.94) -> (141.56, 126.76)

Distance:

195.0 -> 194.46

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.82 4.93 1.82
Low resolution limit 27.99 27.99 1.85
Completeness 90.4 100.0 92.8
Multiplicity 5.9 6.4 6.1
I/sigma 14.0 26.4 -0.2
Rmerge 0.055 0.022 -6.808
CC half 0.998 1.0 0.67
Anomalous completeness 82.2 98.3 90.6
Anomalous multiplicity 3.2 3.2 3.2
Cell 57.85 82.96 95.94 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.915

Sweep:

SWEEP1

Files:

/programs/datagrid/260/b3s10_2_#####.cbf

Images:

1 - 180

Beam:

(141.56, 126.94) -> (141.56, 126.74)

Distance:

195.0 -> 194.47

Spacegroup:

P 21 21 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.56 4.23 1.56
Low resolution limit 41.47 41.49 1.59
Completeness 90.9 99.9 97.7
Multiplicity 6.1 6.0 6.5
I/sigma 9.0 25.4 0.6
Rmerge 0.073 0.023 2.4
CC half 0.998 1.0 0.338
Anomalous completeness 85.3 95.9 96.0
Anomalous multiplicity 3.3 3.3 3.3
Cell 57.84 82.95 95.94 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.915

Sweep:

SWEEP1

Files:

/programs/datagrid/260/b3s10_2_#####.cbf

Images:

1 - 180

Beam:

(141.56, 126.94) -> (141.56, 126.74)

Distance:

195.0 -> 194.71

Spacegroup:

C 2 2 21

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.64 4.45 1.64
Low resolution limit 36.96 36.97 1.67
Completeness 99.6 100.0 99.5
Multiplicity 6.1 6.1 6.3
I/sigma 9.5 22.0 0.9
Rmerge 0.067 0.023 1.128
CC half 0.994 0.985 0.7
Anomalous completeness 98.7 99.4 99.2
Anomalous multiplicity 3.2 3.2 3.2
Cell 83.039 96.031 57.896 90.0 90.0 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.