X-Ray Diffraction data from SrpA + Neu5Gc-Gal disaccharide, source of 5EQ3 structure

Data DOI: 10.15785/SBGRID/242 | ID: 242

5EQ3 Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Iverson Laboratory, Vanderbilt University

Release Date: April 1, 2016

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/242

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/242 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/242 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/242 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/242 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 242 ; shasum -c files.sha'

Storage requirements: 12G

Biological Sample:

SrpA + Neu5Gc-Gal disaccharide

Dataset Type:

X-Ray Diffraction

Subject Composition:

Ligand, Protein

Collection Facility:

APS 21-IDG

Data Creation Date:

June 27, 2015

Related Datasets:

None


Cite this Dataset

Loukachevitch, LV; Iverson, TM. 2016. "X-Ray Diffraction data for: SrpA + Neu5Gc-Gal disaccharide. PDB Code 5EQ3", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/242.

Download Citation

Dataset Description

data with bound ligand

Project Members

Name Additional Roles Affiliation While Working on the Project
Tina M IversonDepositorVanderbilt
Lioudmila V LoukachevitchData CollectorVanderbilt
Tina IversonPIVanderbilt University

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/242/srpasucarb_28.###

Images:

1 - 360

Beam:

(145.3, 155.51) -> (145.3, 155.64)

Distance:

270.0 -> 270.07

Spacegroup:

P 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.97 5.35 1.97
Low resolution limit 85.4 85.48 2.0
Completeness 96.4 97.5 95.6
Multiplicity 3.9 3.9 3.5
I/sigma 5.5 14.5 1.0
Rmerge 0.143 0.064 0.806
CC half 0.987 0.982 0.654
Anomalous completeness 96.0 97.1 94.4
Anomalous multiplicity 2.0 2.0 2.0
Cell 46.933 63.911 90.442 101.741 105.004 90.016

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/242/srpasucarb_28.###

Images:

1 - 360

Beam:

(145.3, 155.51) -> (145.3, 155.6)

Distance:

270.0 -> 269.52

Spacegroup:

C 1 2 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.86 5.05 1.86
Low resolution limit 39.28 39.29 1.89
Completeness 99.0 98.1 94.0
Multiplicity 7.1 6.8 5.4
I/sigma 10.0 26.3 1.0
Rmerge 0.11 0.047 1.745
CC half 0.998 0.998 0.474
Anomalous completeness 98.3 96.3 91.8
Anomalous multiplicity 3.7 3.7 3.7
Cell 174.49 46.98 63.98 90.0 102.11 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/242/srpasucarb_28.###

Images:

1 - 360

Beam:

(145.3, 155.51) -> (145.3, 155.6)

Distance:

270.0 -> 269.62

Spacegroup:

C 1 2 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.85 5.02 1.85
Low resolution limit 56.4 56.43 1.88
Completeness 98.9 97.9 91.7
Multiplicity 7.1 6.8 5.2
I/sigma 9.9 26.2 1.0
Rmerge 0.111 0.047 1.77
CC half 0.998 0.998 0.416
Anomalous completeness 98.1 96.3 89.6
Anomalous multiplicity 3.7 3.7 3.7
Cell 174.49 46.98 63.98 90.0 102.11 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/242/srpasucarb_28.###

Images:

1 - 360

Beam:

(145.3, 155.51) -> (145.3, 155.69)

Distance:

270.0 -> 270.05

Spacegroup:

C 1 2 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.98 5.36 1.98
Low resolution limit 85.57 85.65 2.01
Completeness 99.6 99.7 91.5
Multiplicity 7.3 7.1 6.0
I/sigma 7.1 14.8 1.5
Rmerge 0.142 0.063 1.413
CC half 0.989 0.969 0.832
Anomalous completeness 99.5 99.6 90.9
Anomalous multiplicity 3.8 3.8 3.8
Cell 175.066 47.13 64.303 90.0 102.17 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.