X-Ray Diffraction data from Brucella abortus ChpT phosphotransferase, source of 4QPK structure

Data DOI: 10.15785/SBGRID/149 | ID: 149

Publication DOI: 10.1073/pnas.1503118112

4QPK Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Crosson Laboratory, University of Chicago

Release Date: July 10, 2015

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/149

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/149 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/149 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/149 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/149 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 149 ; shasum -c files.sha'

Storage requirements: 5.6G

Biological Sample:

Brucella abortus ChpT phosphotransferase

Dataset Type:

X-Ray Diffraction

Subject Composition:

Protein

Collection Facility:

LS-CAT, Advanced Photon Source

Data Creation Date:

May 30, 2013

Related Datasets:

None


Cite this Dataset

Herrou, J; Willett, J; Crosson, S. 2015. "X-Ray Diffraction data for: Brucella abortus ChpT phosphotransferase. PDB Code 4QPK", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/149.

Download Citation

Dataset Description

Native ChpT diffraaction dataset

Project Members

Name Additional Roles Affiliation While Working on the Project
Julien HerrouData CollectorUniversity of Chicago
Jonathan WillettData CollectorUniversity of Chicago
Sean CrossonData Collector, Depositor, PIUniversity of Chicago

Reprocessing Instructions

Data were processed in HKL2000 and indexed in space group P43

Reprocessing Data

About Reprocessing

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/149/FL3.###

Images:

1 - 179

Beam:

(145.24, 155.59) -> (145.24, 155.54)

Distance:

200.0 -> 199.94

Spacegroup:

P 41

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.68 4.56 1.68
Low resolution limit 55.22 55.25 1.71
Completeness 100.0 100.0 100.0
Multiplicity 7.5 7.4 7.4
I/sigma 12.3 33.7 1.2
Rmerge 0.08 0.029 1.61
CC half 0.981 0.943 0.326
Anomalous completeness 99.3 99.8 98.4
Anomalous multiplicity 3.8 3.8 3.8
Cell 71.321 71.321 87.24 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/149/FL3.###

Images:

1 - 179

Beam:

(145.24, 155.59) -> (145.24, 155.47)

Distance:

200.0 -> 199.76

Spacegroup:

P 41

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.7 4.61 1.7
Low resolution limit 43.7 43.72 1.73
Completeness 100.0 100.0 100.0
Multiplicity 7.5 7.3 7.5
I/sigma 20.6 68.9 1.1
Rmerge 0.051 0.016 1.726
CC half 0.999 0.999 0.405
Anomalous completeness 99.2 99.8 98.6
Anomalous multiplicity 3.8 3.8 3.8
Cell 71.38 71.38 87.34 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/149/FL3.###

Images:

1 - 179

Beam:

(145.24, 155.59) -> (145.24, 155.46)

Distance:

200.0 -> 199.93

Spacegroup:

P 41

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.69 4.59 1.69
Low resolution limit 50.47 50.5 1.72
Completeness 100.0 100.0 100.0
Multiplicity 7.5 7.3 7.5
I/sigma 20.2 68.7 1.0
Rmerge 0.052 0.016 1.833
CC half 0.999 0.999 0.364
Anomalous completeness 99.2 99.9 98.4
Anomalous multiplicity 3.8 3.8 3.8
Cell 71.38 71.38 87.34 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97856

Sweep:

SWEEP1

Files:

/programs/datagrid/149/FL3.###

Images:

1 - 179

Beam:

(145.24, 155.59) -> (145.24, 155.55)

Distance:

200.0 -> 200.35

Spacegroup:

P 41

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.81 4.91 1.81
Low resolution limit 43.8 43.82 1.84
Completeness 99.7 100.0 94.7
Multiplicity 6.7 7.4 2.9
I/sigma 15.8 38.6 1.2
Rmerge 0.049 0.022 0.858
CC half 0.999 1.0 0.564
Anomalous completeness 96.7 99.9 72.5
Anomalous multiplicity 3.5 3.5 3.5
Cell 71.551 71.551 87.531 90.0 90.0 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.