X-Ray Diffraction data from Benzylsuccinate synthase alpha-beta-gamma complex, source of 4PKF structure

Data DOI: 10.15785/SBGRID/124 | ID: 124

Publication DOI: 10.1073/pnas.1405983111

4PKF Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Drennan Laboratory, Massachusetts Institute of Technology

Release Date: May 21, 2015

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/124

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/124 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/124 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/124 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/124 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 124 ; shasum -c files.sha'

Storage requirements: 6.4G

Biological Sample:

Benzylsuccinate synthase alpha-beta-gamma complex

Dataset Type:

X-Ray Diffraction

Subject Composition:

Protein

Collection Facility:

BCBS (HHMI) 8.2.2, ALS, Berkeley, CA

Data Creation Date:

Oct. 9, 2010

Related Datasets:

None


Cite this Dataset

Funk, MA; Drennan, CL; Drennan, C. 2015. "X-Ray Diffraction data for: Benzylsuccinate synthase alpha-beta-gamma complex. PDB Code 4PKF", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/124.

Download Citation

Dataset Description

Native dataset

Project Members

Name Additional Roles Affiliation While Working on the Project
Michael A FunkData Collector, DepositorMIT
Catherine L DrennanMIT
Catherine DrennanPIMassachusetts Institute of Technology

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

Version:

version unreported

Reprocessing failed.

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.0

Sweep:

SWEEP1

Files:

/programs/datagrid/124/maf049-1_native_###.img

Images:

1 - 360

Beam:

(156.5, 152.6) -> (156.5, 152.59)

Distance:

300.0 -> 297.92

Spacegroup:

I 2 2 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.65 4.48 1.65
Low resolution limit 86.97 87.1 1.68
Completeness 79.0 99.9 31.7
Multiplicity 12.6 13.8 4.3
I/sigma 20.4 43.2 0.8
Rmerge 0.073 0.046 1.218
CC half 0.999 0.999 0.358
Anomalous completeness 77.1 100.0 23.3
Anomalous multiplicity 6.6 6.6 6.6
Cell 113.26 120.2 135.78 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.0

Sweep:

SWEEP1

Files:

/programs/datagrid/124/maf049-1_native_###.img

Images:

1 - 360

Beam:

(156.5, 152.6) -> (156.5, 152.6)

Distance:

300.0 -> 297.56

Spacegroup:

I 2 2 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.65 4.48 1.65
Low resolution limit 86.97 87.1 1.68
Completeness 79.0 99.9 31.7
Multiplicity 12.6 13.8 4.3
I/sigma 20.4 43.2 0.8
Rmerge 0.073 0.046 1.227
CC half 0.999 0.999 0.352
Anomalous completeness 77.1 100.0 23.3
Anomalous multiplicity 6.6 6.6 6.6
Cell 113.26 120.2 135.78 90.0 90.0 90.0

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 1.0

Sweep:

SWEEP1

Files:

/programs/datagrid/124/maf049-1_native_###.img

Images:

1 - 360

Beam:

(156.5, 152.6) -> (156.5, 152.6)

Distance:

300.0 -> 295.79

Spacegroup:

I 2 2 2

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.72 4.67 1.72
Low resolution limit 82.02 82.12 1.75
Completeness 84.6 99.9 42.3
Multiplicity 12.9 13.9 4.8
I/sigma 15.8 31.8 0.9
Rmerge 0.091 0.051 1.78
CC half 0.999 0.999 0.575
Anomalous completeness 83.3 100.0 38.1
Anomalous multiplicity 6.7 6.7 6.7
Cell 112.71 119.598 135.056 90.0 90.0 90.0

License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.