X-Ray Diffraction data from CCM2 HHD in complex with MEKK3 NPB1, source of 4Y5O structure

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Data DOI: 10.15785/SBGRID/563 | ID: 563

Publication DOI: 10.1038/ncomms8937

4Y5O Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB

Boggon Laboratory, Yale University School of Medicine

Release Date: 26 Jan 2018

Data Access Instructions

1. If this dataset is locally available, it should be accessable at /programs/datagrid/563

2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:

'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/563 .' (Harvard Medical School, USA)

Depending on your location, faster access may be available from a Tier 1 site closer to your location

'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/563 .' (Uppsala University, Sweden)

'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/563 .' (Institut Pasteur de Montevideo, Uruguay)

'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/563 .' (Shanghai Institutes for Biological Sciences, China)

3. After the transfer is completed, please issue the following command to verify data integrity:

'cd 563 ; shasum -c files.sha'

Storage requirements: 5.4G

Biological Sample:

CCM2 HHD in complex with MEKK3 NPB1

Dataset Type:

X-Ray Diffraction

Subject Composition:

Protein

Collection Facility:

APS 24-ID-E NE-CAT

Data Creation Date:

24 Jul 2013

Related Datasets:

None


Cite this Dataset

Fisher, OS; Boggon, TJ. 2018. "X-Ray Diffraction data for: CCM2 HHD in complex with MEKK3 NPB1. PDB Code 4Y5O", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/563.

Download Citation

Dataset Description

Native

Project Members

Name Additional Roles Affiliation While Working on the Project
Oriana S FisherData CollectorYale University School of Medicine
Titus J BoggonDepositor, PIYale University School of Medicine

Reprocessing Instructions

none

Reprocessing Data

About Reprocessing

xia2 -2d

xia2 -3d

xia2 -3dii

xia2 -dials
/programs/x86_64-linux/dials/3.12.0/bin.capsules//xia2 pipeline=3d mosflm_beam_centre=152.257996,153.763000 /programs/datagrid//563/ verbose=True multiprocessing.nproc=1 atom=X

Version:

version unreported

Project:

AUTOMATIC

Crystal:

DEFAULT

Sequence Length:

0

Wavelength:

SAD - 0.97914

Sweep:

SWEEP2

Files:

/programs/datagrid/563/OF-TJB6-P01-3_1_###.img

Images:

112 - 273

Beam:

(152.26, 153.76) -> (152.26, 153.53)

Distance:

250.0 -> 255.11

Spacegroup:

P 1 2 1

For AUTOMATIC/DEFAULT/SAD:

ALL LOW HIGH
High resolution limit 1.84 4.99 1.84
Low resolution limit 43.15 43.17 1.87
Completeness 98.2 95.8 90.3
Multiplicity 5.3 5.2 3.2
I/sigma 5.4 18.1 0.1
Rmerge 0.153 0.059 2.946
CC half 0.905 0.945 0.284
Anomalous completeness 92.3 79.7 78.0
Anomalous multiplicity 2.8 2.8 2.8
Cell 43.3 45.36 61.68 90.0 94.72 90.0
/programs/x86_64-linux/dials/3.12.0/bin.capsules//xia2 pipeline=3dii mosflm_beam_centre=152.257996,153.763000 /programs/datagrid//563/ verbose=True multiprocessing.nproc=1 atom=X

Version:

version unreported

Reprocessing failed.

/programs/x86_64-linux/dials/3.12.0/bin.capsules//xia2 pipeline=dials mosflm_beam_centre=152.257996,153.763000 /programs/datagrid//563/ verbose=True multiprocessing.nproc=1 atom=X

Version:

version unreported

Reprocessing failed.


License and Terms of use

License: CC0

Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.