Data DOI: 10.15785/SBGRID/280 | ID: 280
Publication DOI: 10.1021/bi300957f
4EUC Coordinates: Viewer, PDB (RCSB) (PDBe), MMDB
Kappock Laboratory, Purdue University
Release Date: 31 May 2016
1. If this dataset is locally available, it should be accessable at /programs/datagrid/280
2. To download this dataset, please run the following command from your Terminal on a Linux or OS X workstation:
'rsync -av rsync://data.sbgrid.org/10.15785/SBGRID/280 .' (Harvard Medical School, USA)
Depending on your location, faster access may be available from a Tier 1 site closer to your location
'rsync -av rsync://sbgrid.icm.uu.se/10.15785/SBGRID/280 .' (Uppsala University, Sweden)
'rsync -av rsync://sbgrid.pasteur.edu.uy/10.15785/SBGRID/280 .' (Institut Pasteur de Montevideo, Uruguay)
'rsync -av rsync://sbgrid.ncpss.org/10.15785/SBGRID/280 .' (Shanghai Institutes for Biological Sciences, China)
3. After the transfer is completed, please issue the following command to verify data integrity:
'cd 280 ; shasum -c files.sha'
Storage requirements: 12G
Biological Sample:
succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18), E294A mutant bound to dethiaacetyl-CoA
Dataset Type:
X-Ray Diffraction
Subject Composition:
Ligand, Protein
Collection Facility:
beamline 21-ID-G, LS-CAT, APS, Chicago, IL
Data Creation Date:
3 Dec 2011
Related Datasets:
None
Mullins, EA.; Kappock, T. 2016. "X-Ray Diffraction data for: succinyl-CoA:acetate CoA-transferase (EC 2.8.3.18), E294A mutant bound to dethiaacetyl-CoA. PDB Code 4EUC", SBGrid Data Bank, V1, https://doi.org/10.15785/SBGRID/280.
Succinyl-CoA:acetate CoA-transferase (AarCH6-E294A) in complex with dethiaacetyl-CoA
| Name | Additional Roles | Affiliation While Working on the Project |
|---|---|---|
| Elwood A. Mullins | Data Collector | Purdue University |
| T. Joseph Kappock | Depositor, PI | Purdue University |
none
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 0.97856
Sweep:
SWEEP1
Files:
/programs/datagrid/280/dethia3A.###
Images:
1 - 360
Beam:
(145.75, 155.62) -> (145.75, 155.56)
Distance:
200.0 -> 199.25
Spacegroup:
P 21 21 21
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 1.88 | 5.1 | 1.88 |
| Low resolution limit | 43.52 | 43.53 | 1.91 |
| Completeness | 100.0 | 100.0 | 100.0 |
| Multiplicity | 14.7 | 13.1 | 14.8 |
| I/sigma | 10.7 | 41.9 | 0.7 |
| Rmerge | 0.317 | 0.052 | 4.547 |
| CC half | 0.997 | 0.999 | 0.322 |
| Anomalous completeness | 100.0 | 100.0 | 99.9 |
| Anomalous multiplicity | 7.7 | 7.7 | 7.7 |
| Cell | 79.49 | 104.02 | 120.05 | 90.0 | 90.0 | 90.0 |
|---|
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 0.97856
Sweep:
SWEEP1
Files:
/programs/datagrid/280/dethia3A.###
Images:
1 - 360
Beam:
(145.75, 155.62) -> (145.75, 155.56)
Distance:
200.0 -> 199.43
Spacegroup:
P 21 21 21
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 1.88 | 5.1 | 1.88 |
| Low resolution limit | 60.03 | 60.06 | 1.91 |
| Completeness | 100.0 | 100.0 | 100.0 |
| Multiplicity | 14.7 | 13.1 | 14.8 |
| I/sigma | 10.7 | 41.9 | 0.7 |
| Rmerge | 0.317 | 0.052 | 4.562 |
| CC half | 0.997 | 0.999 | 0.317 |
| Anomalous completeness | 100.0 | 99.9 | 99.9 |
| Anomalous multiplicity | 7.7 | 7.7 | 7.7 |
| Cell | 79.49 | 104.02 | 120.05 | 90.0 | 90.0 | 90.0 |
|---|
Version:
version unreported
Project:
AUTOMATIC
Crystal:
DEFAULT
Sequence Length:
0
Wavelength:
SAD - 0.97856
Sweep:
SWEEP1
Files:
/programs/datagrid/280/dethia3A.###
Images:
1 - 360
Beam:
(145.75, 155.62) -> (145.75, 155.65)
Distance:
200.0 -> 199.22
Spacegroup:
P 21 21 21
For AUTOMATIC/DEFAULT/SAD:
| ALL | LOW | HIGH | |
|---|---|---|---|
| High resolution limit | 1.43 | 3.88 | 1.43 |
| Low resolution limit | 119.96 | 120.39 | 1.46 |
| Completeness | 99.7 | 100.0 | 93.8 |
| Multiplicity | 12.4 | 14.4 | 7.1 |
| I/sigma | 11.6 | 10.6 | 25.7 |
| Rmerge | 0.18 | 0.334 | 0.108 |
| CC half | 0.964 | 0.986 | 0.048 |
| Anomalous completeness | 99.3 | 100.0 | 91.2 |
| Anomalous multiplicity | 6.4 | 6.4 | 6.4 |
| Cell | 79.468 | 103.874 | 119.963 | 90.0 | 90.0 | 90.0 |
|---|
License: CC0
Terms: Our Community Norms as well as good scientific practices expect that proper credit is given via citation. Please use the data citation, as generated by the SBGrid Data Bank.
